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Noncontact Measurements of Heat Capacity, Thermal Conductivity and Emissivity of High Temperature Melts by Modulated Laser Calorimetry

作者:HIROYUKI FUKUYAMA;HIDEKAZU KOBATAKE;TAKAO TSUKADA;

作者单位:Institute of Multidisciplinary Research for Advanced Materials (TMRAM), Tohoku University 2-1-1 Katahira, Aoba-ku, Sendai-shi, Miyagi 980-8577

刊名:Journal of the Technical Association of Refractories

ISSN:0285-0028

出版年:2008-01-05

卷:28

期:4

起页:253

止页:258

分类号:TQ175

语种:英文

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内容简介

We have developed a new modulated laser calorimetry that can suppress the convection in a levitated molten sample by superimposing a static magnetic field. We have succeeded in measuring the molar heat capacity, thermal conductivity, and hemispherical total emissivity of molten silicon over a broad temperature range. Our technique has the advantage that it is free from crucible contamination and can measure over a wide temperature range that includes super-cooling. In the near future, we would like to apply this method to other metals by improvement of the experimental apparatus and through further verification of our method. We hope that the present method will become a standard to determine the thermal properties of high temperature molten materials. We are happy to receive your opinions.

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